Synthesis of new polymers containing 1,2,3-triazole units from poly(vinylchloride) via "click” chemistry catalyzed by copper iodide and its application in extraction of nitrates and metals contained in wastewater

Abid Ouerghui; Mokthar Dardouri; Noomene Sleimi; Abir Bel Hadj Amor; Faycel Ammari; Christian Girard

doi:10.14314/polimery.2019.1.1

Published : 2021-01-12

Vol. 64 No. 1 (2019)

Synthesis of new polymers containing 1,2,3-triazole units from poly(vinylchloride) via "click” chemistry catalyzed by copper iodide and its application in extraction of nitrates and metals contained in wastewater

Abid Ouerghui Mokthar Dardouri Noomene Sleimi Abir Bel Hadj Amor Faycel Ammari Christian Girard

DOI: https://doi.org/10.14314/polimery.2019.1.1

Abstract

New polymers with potential application in a waste water purification from inorganic contaminants were synthesized via a chemical modification of poly(vinyl chloride) by "click” method based on copper(I)-catalyzed Huisgen reaction. The structure of the resulting polymers containing 1,4-disubstituted triazole units was confirmed by infrared spectroscopy (ATR-FTIR), nitrogen elemental analysis and differential thermal analysis (DTA). The obtained polymers were subsequently used in the elimination of nitrate ions and metalions from the wastewater of Beja region (Tunisia). It was found that new polymers were most efficient in capturing of zinc ions, the average extraction percentage of Zn2+ was 28%, while the average extraction percentage of nitrates did not exceed 12.5%. The selectivity of the binding of investigated ions can be arranged in the following order: Zn2+> NO3–> Ca2+> Mg2+.

Keywords

"click” chemistry ; poly(vinylchloride) ; 1, 4-triazoles ; extraction ; nitrates ; metals ; wastewater reakcje „click” ; poli(chlorek winylu) ; 1, 4-triazole ; ekstrakcja ; azotany ; metale ; ścieki

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Ouerghui, A., Dardouri, M., Sleimi, N., Bel Hadj Amor, A., Ammari, F., & Girard, C. (2021). Synthesis of new polymers containing 1,2,3-triazole units from poly(vinylchloride) via "click” chemistry catalyzed by copper iodide and its application in extraction of nitrates and metals contained in wastewater. Polimery, 64(1), 3-11. https://doi.org/10.14314/polimery.2019.1.1

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Abid Ouerghui ouerghiabid@gmail.com

Affiliation
Unité de Technologies Chimiques et Biologiques pour la Santé, UMR 8258 CNRS/U 1022 Inserm, Ecole Nationale Supérieure de Chimie de Paris, 11 rue Pierre et Marie Curie, 75005 Paris, France

Mokthar Dardouri

Affiliation
Université de Carthage, Faculté des Sciences de Bizerte, Jarzouna, Bizerte 7021, Tunisia

Noomene Sleimi

Affiliation
Université de Carthage, Faculté des Sciences de Bizerte, Jarzouna, Bizerte 7021, Tunisia

Abir Bel Hadj Amor

Affiliation
Université de Carthage, Faculté des Sciences de Bizerte, Jarzouna, Bizerte 7021, Tunisia

Faycel Ammari

Affiliation
Université de Carthage, Faculté des Sciences de Bizerte, Jarzouna, Bizerte 7021, Tunisia

Christian Girard

Affiliation
Unité de Technologies Chimiques et Biologiques pour la Santé, UMR 8258 CNRS/U 1022 Inserm, Ecole Nationale Supérieure de Chimie de Paris, 11 rue Pierre et Marie Curie, 75005 Paris, France