Novel N,N’-bis(2,4-dimethoxybenzylidene)ethylenediamine PVC membrane electrode for the potentiometric iron selective sensor based on Schiff base ligand

Sachin Kumar; Susheel Sandhu; Angik K.  Patel; Ketankumar H.  Parmar

doi:10.14314/polimery.2022.5.2

Published : 2022-06-10

Vol. 67 No. 5 (2022)

Novel N,N’-bis(2,4-dimethoxybenzylidene)ethylenediamine PVC membrane electrode for the potentiometric iron selective sensor based on Schiff base ligand

Sachin Kumar https://orcid.org/0000-0002-9131-582X Susheel Sandhu https://orcid.org/0000-0001-7944-8593 Angik K. Patel https://orcid.org/0000-0001-6746-895X Ketankumar H. Parmar https://orcid.org/0000-0002-8886-7711

DOI: https://doi.org/10.14314/polimery.2022.5.2

Abstract

N,N’-bis(2,4-dimethoxybenzylidene)ethylenediamine was synthesized and used as a membrane carrier to create a novel poly(vinyl chloride) membrane potentiometric sensor that is selective especially for Fe3+ ions. The super-Nernstian slope of the projected sensor was 19.5 mV per decade over a concentration range of 7.3·10−8 –1·10−1 M having detection limit at 7.3·10−8 M. The sensor displayed a linear potential response for the detection of Fe3+ ions in about 30 seconds, and it had a lifespan of no less than 9 weeks without lacking any potential divergence. The selected sensor showed high selectivity in water solutions in relation to Fe3 + ions, even in the presence of other metal cations in the pH range of 3.6–10.

Keywords

Fe3 ions ; ion-selective electrode ; PVC membrane ; potentiometry ; Schiff base jony Fe3 ; elektrody jonoselektywne ; membrana PVC ; potencjometria, ; zasada Schiffa

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Kumar, S., Sandhu, S., Patel, A. K. ., & Parmar, K. H. . (2022). Novel N,N’-bis(2,4-dimethoxybenzylidene)ethylenediamine PVC membrane electrode for the potentiometric iron selective sensor based on Schiff base ligand. Polimery, 67(5), 197-204. https://doi.org/10.14314/polimery.2022.5.2

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