Application of in-line rheological measurements for characterization of polypropylene/opoka rock powder composites

Arkadiusz Kloziński; Paulina Jakubowska; Joanna E. Przybylska; Robert Przekop

doi:10.14314/polimery.2019.4.6

Published : 2021-01-12

Vol. 64 No. 4 (2019)

Application of in-line rheological measurements for characterization of polypropylene/opoka rock powder composites

Arkadiusz Kloziński Paulina Jakubowska Joanna E. Przybylska Robert Przekop

DOI: https://doi.org/10.14314/polimery.2019.4.6

Abstract

The rheological properties of the composites of polypropylene (PP) with a new natural powder hybrid filler – carbonate-silicate rock called opoka – were investigated. Opoka rock is industrial waste originating (as a subsieve fraction) from the production of sorbents used in water treatment processes. The effect of opoka addition (1, 5 and 10 wt %) on the processability of PP was determined during the extrusion process using an in-line measuring stand. The testing instrument was an extruder rheometer equipped with a rheological measuring head with exchangeable dies. Cylindrical measuring dies with a radius of 1.5 mm and a length of L = 20, 30, 40 and 50 mm, respectively, were used in the measurements. The rheological parameters of the composites were determined based on the Ostwald-de-Waele power--law model at a temperature of 230 °C. The effect of the addition of opoka on the extruder operating characteristic, flow curves, viscosity curves, and the values of power law index (n), consistency factor (K), mass flow rate (MFR) and volume flow rate (MVR) have been determined.

Keywords

polypropylene ; polymer composites ; opoka ; powder filler ; natural filler ; hybrid filler ; in-line rheology ; viscosity ; viscosity curve polipropylen ; kompozyty polimerowe ; opoka ; napełniacz proszkowy ; napełniacz naturalny ; napełniacz hybrydowy ; reologia in-line ; lepkość ; krzywa lepkości

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Kloziński, A., Jakubowska, P., Przybylska, J. E., & Przekop, R. (2021). Application of in-line rheological measurements for characterization of polypropylene/opoka rock powder composites. Polimery, 64(4), 282–289. https://doi.org/10.14314/polimery.2019.4.6

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Arkadiusz Kloziński Arkadiusz.Klozinski@put.poznan.pl

Affiliation
Poznan University of Technology, Institute of Chemical Technology and Engineering, Berdychowo 4, 60-965 Poznań, Poland

Paulina Jakubowska

Affiliation
Poznan University of Technology, Institute of Chemical Technology and Engineering, Berdychowo 4, 60-965 Poznań, Poland

Joanna E. Przybylska

Affiliation
Poznan University of Technology, Institute of Chemical Technology and Engineering, Berdychowo 4, 60-965 Poznań, Poland

Robert Przekop

Affiliation
University of Adam Mickiewicz in Poznan, Center for Advanced Technology, Umultowska 89c, 61-614 Poznań, Poland