Comparison of thermal, structural and morphological properties of poly(l-lactide) and poly(l-lactide)/ hydroxyapatite microspheres for laser sintering processes

Anna Krokos; Agnieszka Bondyra; Ryszard Kwiatkowski; Piotr Gruber; Michał Olejarczyk; Bogusz Stępak; Paulina Dzienny; Bartłomiej Kryszak; Małgorzata Gazińska; Arkadiusz Antończak

doi:10.14314/polimery.2020.9.2

Published : 2020-12-16

Vol. 65 No. 9 (2020)

Comparison of thermal, structural and morphological properties of poly(l-lactide) and poly(l-lactide)/ hydroxyapatite microspheres for laser sintering processes

Anna Krokos Agnieszka Bondyra Ryszard Kwiatkowski Piotr Gruber Michał Olejarczyk Bogusz Stępak Paulina Dzienny Bartłomiej Kryszak Małgorzata Gazińska Arkadiusz Antończak

DOI: https://doi.org/10.14314/polimery.2020.9.2

Abstract

A comparison of poly(l-lactide) (PLLA) and poly(l-lactide)/hydroxyapatite (PLLA/HAp) biocomposite microspheres fabricated by emulsion solvent evaporation technique designed for laser sintering (LS) applications is presented. Key properties such as thermal and structural as well as geometry, size distribution and powder flowability, which are crucial for this technique, are characterized to validate the applicability of microspheres for LS. The biocomposite microspheres turns out to be more suitable for the LS process than PLLA due to the higher thermal stability, broader sintering window and higher powder flowability.

Keywords

poly(l-lactide) ; hydroxyapatite ; microspheres ; biocomposite ; laser sintering ; additive manufacturing ; biomedical applications ; sintering window ; powder flowability poli(l-laktyd) ; hydroksyapatyt ; mikrosfery ; biokompozyt ; spiekanie laserowe ; techniki addytywne ; zastosowania biomedyczne ; okno spiekania ; sypkość proszku

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Krokos, A., Bondyra, A., Kwiatkowski, R., Gruber, P., Olejarczyk, M., Stępak, B., Dzienny, P., Kryszak, B., Gazińska, M., & Antończak, A. (2020). Comparison of thermal, structural and morphological properties of poly(l-lactide) and poly(l-lactide)/ hydroxyapatite microspheres for laser sintering processes. Polimery, 65(9), 605-612. https://doi.org/10.14314/polimery.2020.9.2

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Anna Krokos

Affiliation
Wroclaw University of Science and Technology, Faculty of Chemistry, Polymer Engineering and Technology Division, C.K. Norwida 4/6, 50-373 Wrocław, Poland

Agnieszka Bondyra

Affiliation
Wroclaw University of Science and Technology, Faculty of Chemistry, Polymer Engineering and Technology Division, C.K. Norwida 4/6, 50-373 Wrocław, Poland

Ryszard Kwiatkowski

Affiliation
University of Bielsko-Biała, Institute of Textile Engineering and Polymer Materials, Willowa 2, 43-309 Bielsko-Biała, Poland

Piotr Gruber

Affiliation
Wroclaw University of Science and Technology, Faculty of Mechanical Engineering/Centre of Advanced Manufacturing Technologies – Fraunhofer Project Center (CAMT-FPC), Łukasiewicza 5, 50-371 Wrocław, Poland.

Michał Olejarczyk

Affiliation
Wroclaw University of Science and Technology, Faculty of Mechanical Engineering/Centre of Advanced Manufacturing Technologies – Fraunhofer Project Center (CAMT-FPC), Łukasiewicza 5, 50-371 Wrocław, Poland.

Bogusz Stępak

Affiliation
Wroclaw University of Science and Technology, Faculty of Electronics, Laser and Fibre Electronics Group, Wybrzeże Wyspiańskiego 27, 50-370 Wrocław, Poland

Paulina Dzienny

Affiliation
Wroclaw University of Science and Technology, Faculty of Electronics, Laser and Fibre Electronics Group, Wybrzeże Wyspiańskiego 27, 50-370 Wrocław, Poland

Bartłomiej Kryszak

Affiliation
Wroclaw University of Science and Technology, Faculty of Chemistry, Polymer Engineering and Technology Division, C.K. Norwida 4/6, 50-373 Wrocław, Poland

Małgorzata Gazińska

Affiliation
Wroclaw University of Science and Technology, Faculty of Chemistry, Polymer Engineering and Technology Division, C.K. Norwida 4/6, 50-373 Wrocław, Poland

Arkadiusz Antończak arkadiusz.antonczak@pwr.edu.pl

Affiliation
Wroclaw University of Science and Technology, Faculty of Electronics, Laser and Fibre Electronics Group, Wybrzeże Wyspiańskiego 27, 50-370 Wrocław, Poland